kiloclave - 实验室和中试中使用的压力反应釜

实验室压力反应釜系统

反应器容积: 0.5-20.0 升
工作压力:-1 (FV)~ + 60 / 200 bar
工作温度:-20 ° C ~ + 250 ° C
材料: 不锈钢、 哈氏合金、 搪玻璃

其他材料、 压力 & 温度都可定制

该多用途压力反应釜系统可适用大型不锈钢压力釜体。釜体液压提升与倾斜功能使打开和闭合的釜体清洗变的很容易。其安全功能保障压力下的反应安全。

不锈钢或高抗酸性的哈氏合金反应釜体。不锈钢压力容器安装视窗玻璃可实现高压下的视觉过程控制和监测。可配备各种由低到高扭矩的磁驱耦合驱动马达,确保从低到高粘度的介质都能高效的混合和搅拌以及有优秀的热传导性能。

Kiloclave 系统的模块设置允许你在任何时候进行功能变更或升级新的使用功能。

种类繁多的配件用于液体 / 固体/气体加料,快速开合装置,和催化剂篮等。和我们沟通来确认您的特殊需要的正确配置。

包装 / 选项

标准配置

  • 支架有液压升降和倾倒功能
  • 不锈钢 / 哈氏合金压力釜体有对应的搅拌轴、 搅拌桨、 挡板、 Pt 100 和底阀
  • 盖板有 7 格开口和标准设置:
  • 欧美标准的破裂阀、 压力表和 2个阀门
  • 工具和备件

标准可选项

有恒温加热夹套的压力釜体

Type 3
金属
0.5、 1.0、 2.0、 3.0、 5.0、
10.0 20.0 升
250 ° C
60 bar (20 bar 10.0 升, 10 bar 20.0 升)

 

Type 4
金属/视镜玻璃
1.0, 1.5, 2.0, 3.0, 5.0, 10.0 20.0 升
250 ° C
60 bar (20 bar 10.0 升, 10 bar 20.0 升)

 

电加热和水冷却压力釜体

Type 3E
金属
 

0.5, 1.0, 1.5, 2.0, 3.0, 5.0,
10.0, 20.0 升r
250°C
60 bar (20 bar 10.0 升, 10 bar 20.0 升)

 

Type 4E
金属/视镜玻璃

1.0, 1.5, 2.0, 3.0, 5.0, 10.0 20.0 升
250°C
60 bar (20 bar 10.0 升, 10 bar 20.0 升 )

 

 

btc
PID 温度控制器
type 3E 和 4E 釜体
 

 

案例

Customer references

"For carbonization, we have chosen the Buchi kiloclave Type 3E with a Cyclone 300 drive as stirrer agitator. The design of the reactor stand allows easy filling and emptying by single person. The individual components can be cleaned easily. Two stainless steel vessels with 0.5 liter and 5 liter are available as reactor vessels. For special reaction experiments in the acidic range by adding organic or mineral acids, a 1 liter reactor made of Hastelloy® is used."
Gabriel Gerner, Research assistant, Zurich University of Applied Sciences ZHAW, Wädenswil

Read here the case study Sustainable coal production in Buchi kiloclave type 3E.

"Our emulsion polymerization process is very difficult to simulate at the laboratory scale. The process runs at moderately high temperature and elevated pressure. High-shear agitation is critical to product quality. We have struggled to identify a pilot reactor that provided just what we need.  The available systems either cannot achieve the elevated pressure or are designed for extreme pressure, making them extremely bulky and costly. We had begun enlisting custom equipment manufacturers until we came across the Buchi kiloclave system, which was a good fit for us. With some simple, cost effective, customization, the kiloclave has proven to be the perfect pilot reactor for our process optimization."
Mark G. Stevens, PhD., Sr. Manager, Engineering Design and Development, Dentsply Sirona, Restoratives 

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